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Automated headspace gas chromatographic analysis of faecal short-chain fatty acids

Research output: Contribution to journalArticle

Standard

Automated headspace gas chromatographic analysis of faecal short-chain fatty acids. / Stansbridge, E.; Mills, Graham; Walker, V.

In: Journal of Chromatography B: Biomedical Sciences and Applications, Vol. 621, No. 1, 17.11.1993, p. 7-13.

Research output: Contribution to journalArticle

Harvard

Stansbridge, E, Mills, G & Walker, V 1993, 'Automated headspace gas chromatographic analysis of faecal short-chain fatty acids', Journal of Chromatography B: Biomedical Sciences and Applications, vol. 621, no. 1, pp. 7-13. https://doi.org/10.1016/0378-4347(93)80070-K

APA

Stansbridge, E., Mills, G., & Walker, V. (1993). Automated headspace gas chromatographic analysis of faecal short-chain fatty acids. Journal of Chromatography B: Biomedical Sciences and Applications, 621(1), 7-13. https://doi.org/10.1016/0378-4347(93)80070-K

Vancouver

Stansbridge E, Mills G, Walker V. Automated headspace gas chromatographic analysis of faecal short-chain fatty acids. Journal of Chromatography B: Biomedical Sciences and Applications. 1993 Nov 17;621(1):7-13. https://doi.org/10.1016/0378-4347(93)80070-K

Author

Stansbridge, E. ; Mills, Graham ; Walker, V. / Automated headspace gas chromatographic analysis of faecal short-chain fatty acids. In: Journal of Chromatography B: Biomedical Sciences and Applications. 1993 ; Vol. 621, No. 1. pp. 7-13.

Bibtex

@article{a7cbe1acc78a4daa9965fb64b1a59a29,
title = "Automated headspace gas chromatographic analysis of faecal short-chain fatty acids",
abstract = "A method was developed and validated for analysis of faecal short-chain fatty acids using automated headspace gas chromatography. Quantification was by standard addition. Ghosting was minimized by lining the transfer tube from the headspace sampler to the gas chromatograph with deactivated fused silica and addition of formic acid to sample vials. Saturation of samples with lithium sulphate increased recoveries. The method was used to analyse small amounts of faecal matter collected from premature babies. Advantages of the technique are rapid, accurate, analysis of faecal specimens in batches, with minimum sample preparation.",
author = "E. Stansbridge and Graham Mills and V. Walker",
year = "1993",
month = "11",
day = "17",
doi = "10.1016/0378-4347(93)80070-K",
language = "English",
volume = "621",
pages = "7--13",
journal = "Journal of Chromatography B: Biomedical Sciences and Applications",
issn = "1387-2273",
publisher = "Elsevier BV",
number = "1",

}

RIS

TY - JOUR

T1 - Automated headspace gas chromatographic analysis of faecal short-chain fatty acids

AU - Stansbridge, E.

AU - Mills, Graham

AU - Walker, V.

PY - 1993/11/17

Y1 - 1993/11/17

N2 - A method was developed and validated for analysis of faecal short-chain fatty acids using automated headspace gas chromatography. Quantification was by standard addition. Ghosting was minimized by lining the transfer tube from the headspace sampler to the gas chromatograph with deactivated fused silica and addition of formic acid to sample vials. Saturation of samples with lithium sulphate increased recoveries. The method was used to analyse small amounts of faecal matter collected from premature babies. Advantages of the technique are rapid, accurate, analysis of faecal specimens in batches, with minimum sample preparation.

AB - A method was developed and validated for analysis of faecal short-chain fatty acids using automated headspace gas chromatography. Quantification was by standard addition. Ghosting was minimized by lining the transfer tube from the headspace sampler to the gas chromatograph with deactivated fused silica and addition of formic acid to sample vials. Saturation of samples with lithium sulphate increased recoveries. The method was used to analyse small amounts of faecal matter collected from premature babies. Advantages of the technique are rapid, accurate, analysis of faecal specimens in batches, with minimum sample preparation.

U2 - 10.1016/0378-4347(93)80070-K

DO - 10.1016/0378-4347(93)80070-K

M3 - Article

VL - 621

SP - 7

EP - 13

JO - Journal of Chromatography B: Biomedical Sciences and Applications

JF - Journal of Chromatography B: Biomedical Sciences and Applications

SN - 1387-2273

IS - 1

ER -

ID: 246259